Скачать или смотреть Experiment #11 Synthesis of KBArF4, Cp2FeBArF4, and AgBArF4

This laboratory experiment demonstrates the synthesis of KBArF4 through the use of a Grignard reaction. The experiment then describes the use of the KBArF4 to generate Cp2FeBArF4 (undergraduate students) and AgBarF4 (graduate students). This experiment is completed over four lab periods.

For the generation of KBArF4 using a Grignard reaction (Lab Period #1), please start here: 0:18

For the purification procedure in the preparation of KBArF4 (Lab Period #2), please start here: 15:20

For the procedure in generating a solid from an oil of KBArF4 (Lab Period #3), please start here: 24:26

For a description on the generation of Cp2FeBArF4 (Lab Period #4 for undergraduate students), please start here: 29:47

For a description on the generation of AgBArF4 (Lab Period #4 for graduate students), please start here: 46:02