Lec-9 || Fast Atom Bombardment (FAB) || Neutral atom bombardment || Matrix || Direct Probe method

#massspectrometry
Lec-1 || Intro to Mass Spectrometry || Molecular ion peak || Basic principle || m/e value
   • Lec-1 || Intro to Mass Spectrometry |...  
Lec-2 || Parts of Mass spectrometer | Instrumentation | Functions of different parts of spectrometer
   • Lec-2 || Parts of Mass spectrometer |...  
Lec-3 || Sample introduction in Mass Spectrometer || Nature of analyte || Type of sample
   • Lec-3 || Sample introduction in Mass ...  
Lec-4 || Ionization techniques || El || CI || FAB || FD|| MALDI || ESI || TSI || APCI || APPI
   • Lec-4 || Ionization techniques || El ...  
Lec-5 || Electron Ionization (EI) || Instrumentation || Advantages || Disadvantages
   • Lec-5 || Electron Ionization (EI) || ...  
Lec-6 || Chemical ionization || Mechanism of CI || Ionizing gases || Advantages || Disadvantages
   • Lec-6 || Chemical ionization || Mecha...  
Lec-7 || Direct Analysis in Real Time (DART) || Open air Ionization technique|| Helium as carrier
   • Lec-7 || Direct Analysis in Real Time...  
Lect-8 || Field desorption Ionization || Evaporative Tech || Soft Ionization || Anode emitters
   • Lect-8 || Field desorption Ionization...  
Lec-9 || Fast Atom Bombardment (FAB) || Neutral atom bombardment || Matrix || Direct Probe method
   • Lec-9 || Fast Atom Bombardment (FAB) ...  
Lec-10 || Matrix-Assisted Laser Desorption Ionization (MALDI) || Types & Properties of matrix
   • Lec-10 || Matrix-Assisted Laser Desor...  
Lec-11 || Electro Spray Ionization (ESI) || Evaporative|| Soft Ionization|| Nebulization to aerosol
   • Lec-11 || Electro Spray Ionization (E...  
Lec-12 || Thermo Spray Ionization (TSI) || Evaporative & Soft ionization || HPLC Coupled TSI
   • Lec-12 || Thermo Spray Ionization (TS...  
Lec-13 || Atmospheric Pressure Chemical Ionization (APCI)|| Soft Ionization || Corona Discharge Lamp
   • Lec-13 || Atmospheric Pressure Chemic...  
Lec-14 || Atmospheric Pressure Photo Ionization (APPI)|| Soft ionization || Xenon lamp| Evaporative
   • Lec-14 || Atmospheric Pressure Photo ...  
Lec#15 || Molecular ion peak || Parent ion peak || Identification & stability of molecular ion peak
   • Lec#15 || Molecular ion peak || Paren...  
Lec-16 || Isotopic peaks in mass spectrometry || Relative intensities of isotopic peaks of Cl and Br
   • Lec-16 || Isotopic peaks in mass spec...  
Lec#17 || Metastable ion peak || Fragmentation in field free region || Mass spectrometry
   • Lec#17 || Metastable ion peak || Frag...  
Lec#18 || Fragmentation || Types of peaks || Base peak || Daughter peaks || Mass spectrometry
   • Lec#18 || Fragmentation || Types of p...  
Lec-19 || Stevenson rule || Ionization of molecule || Fragmentation and stability of carbocation
   • Lec-19 || Stevenson rule || Ionizatio...  
Lec-20 || Types of bond cleavage in Mass spectrometry || Charge and radical site initiated cleavage
   • Lec-20 || Types of bond cleavage in M...  
Lec-21 || McLafferty Rearrangement || All classes which give Mclafferty Rearrangement
   • Lec-21 || McLafferty Rearrangement ||...  
Lec-22 || Retro Diels Alder Reaction || Fragmentation in cylcoalkenes || Dienes || Dienophiles
   • Lec-22 || Retro Diels Alder Reaction ...  
Lec-23 || Fragmentation pattern in alkanes || Stability of carbocations & Molecular ion peaks
   • Lec-23 || Fragmentation pattern in al...  
Lec-24 || Fragmentation pattern of cycloalkanes & bicycloalkanes || Intensity of molecular ion peak
   • Lec-24 || Fragmentation pattern of cy...  
Lec-25 || Fragmentation pattern of alkene, cycloalkene & alkyne | Mass spectrum of limonene & ionone
   • Lec-25 || Fragmentation pattern of al...  
Lec-26 || Mass fragmentation in aromatic hydrocarbons || Tropylium ion || Mclafferty rearrangement
   • Lec-26 || Mass fragmentation in aroma...  
Lec-27 || Mass Fragmentation Pattern in alcohols, phenols, cyclic alcohols & thio-alcohols
   • Lec-27 || Mass Fragmentation Pattern ...  
Lec-28 || Mass fragmentation pattern of aldehydes || Peaks in mass spectrum of aldehydes
   • Lec-28 || Mass fragmentation pattern ...  
Lec-29 || Mass fragmentation of ketones || Mclafferty rearrangement || Mass spectrum of ketones
   • Lec-29 || Mass fragmentation of keton...  
Lec-30 || Fragmentation pattern of esters || Methyl & higher esters || MacLafferty rearrangement
   • Lec-30 || Fragmentation pattern of es...  
Lec-31 || Mass fragmentation pattern of carboxylic acids | McLafferty rearrangement | Alpha cleavage
   • Lec-31 || Mass fragmentation pattern ...  
Lec-32 || Mass fragmentation pattern of amines || Alpha cleavage || Cyclic & aromatic amines
   • Lec-32 || Mass fragmentation pattern ...  
Lec-33 || Mass fragmentation pattern of amides || McLafferty rearrangement || Acetanilide
   • Lec-33 || Mass fragmentation pattern ...  
Lec-34 || Mass Fragmentation Pattern of Nitriles || McLafferty rearrangement || Nitrogen rule
   • Lec-34 || Mass Fragmentation Pattern ...  
Lec-35 || Mass Fragmentation pattern of nitro compounds || Nitropropane || Nitrobenzene
   • Lec-35 || Mass Fragmentation pattern ...  
Lec-36 || Mass fragmentation pattern of alkyl halides || Alpha cleavage || Isotopic peaks
   • Lec-36 || Mass fragmentation pattern ...  



Fast Atom Bombardment (FAB)
Neutral atom bombardment
Matrix
Direct Probe method
Matrix types
Soft ionization
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