Making The Sweetest Compound Known (Lugduname)

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Literature:
test in pigs
https://sci-hub.se/https://doi.org/10...

2,3-dihydroxybenzaldehyde via o-vanillin + acetic acid + hbr
https://sci-hub.se/https://doi.org/10...

Methylenedioxy aldehyde
https://sci-hub.se/https://doi.org/10...

Oxime
http://koreascience.or.kr/article/JAK...
https://www.rsc.org/suppdata/ob/c2/c2...

Oxime & Amine
https://onlinelibrary.wiley.com/actio...

Biphasic isothiocyanate synth
https://sci-hub.se/https://doi.org/10...

T-Bu Gly (for boiling point)
https://www.orgsyn.org/demo.aspx?prep...

review about thioureas to guanidines
https://www.arkat-usa.org/get-file/19...

HgCl2 guanylation
https://sci-hub.se/https://doi.org/10...
https://www.sciencedirect.com/science...

(alternative) aq phosphoric acid deprotect of t-bu ester
https://sci-hub.se/https://doi.org/10...

trisub guanidine acetic acids
https://pubs.acs.org/doi/pdf/10.1021/...
https://sci-hub.se/https://doi.org/10...

synth of trisub guanidines (only with aryl-carbonyl group)
https://pubmed.ncbi.nlm.nih.gov/30913...
https://sci-hub.se/10.1016/j.ejmech.2...

makes disubstituted guanidines
https://sci-hub.se/https://doi.org/10...
https://pubs.acs.org/doi/suppl/10.102...

Makes some guanidines, purifies them with flash column using 100 DCM 1 Methanol
https://sci-hub.se/https://doi.org/10...

Guanidines, Mentions regular column chromatography with 100% EtOAc
https://sci-hub.se/https://doi.org/10...

Mentions columning with 50% EtOAc
https://www.sciencedirect.com/science...
https://ars.els-cdn.com/content/image...

Patent for these sweeteners
https://worldwide.espacenet.com/paten...