Making Dibenzo[a,e]cyclooctene - an Emerging Ligand?

Описание к видео Making Dibenzo[a,e]cyclooctene - an Emerging Ligand?

In this video I am synthesizing the ligand dibenzo[a,e[cyclooctene, employing various methods including cold finger sublimation to purify the products!

Xylene bromination:
http://www.orgsyn.org/demo.aspx?prep=...

Dibenzo[a,e]cyclooctene synthesis:
http://www.orgsyn.org/demo.aspx?prep=...

More information about NBS bromination:
https://chem.libretexts.org/Bookshelv...
https://en.wikipedia.org/wiki/Wohl%E2...

Synthesis of some complexes with the ligand (where I got structure from):
doi:10.1016/j.ica.2007.12.007

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