Profex XRD: First Rietveld Refinement with Profex

We perform a first Rietveld refinement.

Download the example dataset:
https://www.profex-xrd.org/wp-content...

0:23 Results of search-match phase identification from previous episode
0:41 Create the refinement project
3:05 Explanation of the refinement control file (*.sav)
6:18 Running the refinement
8:45 Explanation of the convergence progress graph
11:25 Analyze the fit
12:59 Edit a structure file
14:11 Explanation of the STR file format
18:47 Using the context help
21:25 Releasing structural parameters for refinement
32:58 Repeat the refinement with the modified structure file
34:02 Add more phases to the refinement
37:58 Refine anisotropic peak shape
41:10 Explanation of refinement results
46:13 Export of refinement results
49:08 Refined chemical composition
51:02 Generate refinement report
53:05 Export of the graph to a pixel image or in SVG format
57:14 Edit SVG files in Inkscape
58:45 Closing remarks